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Table 3 Interday and Intraday precision results for GC-MS

From: Development and validation of the method for the detection of glimepiride via derivatization employing N-methyl-N-(trimethylsilyl) trifluoroacetamide using gas chromatography-mass spectrometry

Concentration (ng/ml)

Intraday

Interday

Mean (x)

X + SD

Precision (RSD) (%)

Mean (x)

X + SD

Precision (RSD) (%)

500

317.2

317.2 + 3.162

0.74

315

315 + 3.16

0.70

1000

996.4

996.4 + 7.82

0.75

985.2

985.2 + 7.85

0.77

1500

1327.6

1327.6 + 11.01

0.82

1320.4

1320.4 + 11.34

0.85

2000

1987.6

1987.6 + 15.07

0.78

1980.2

1980.2 + 15.4

0.79

2500

2314.4

2314.4 + 17.32

0.99

2307.4

2307.4 + 16.31

1.003