Table 1 GC-PFC parameters
Temperature 1 (°C) | Rate (°C/min) | Temperature 2 (°C) | Hold (min) |
|---|---|---|---|
GC temperature program | |||
110 | – | 110 | 2 |
110 | 15 | 320 | 30 |
PTV temperature program | |||
0 | – | 0 | 0.1 |
0 | 700 | 330 | 4 |
330 | 100 | 250 | 41.9 |
Temperature of the fraction collector (the box) | |||
330 °C throughout the fraction process | |||